2,5-二甲氧基苯异氰酸酯合成路线 （共 6 条）
反应条件
diphenyl phosphoryl azide; triethylamine T=80°C; Curtius Rearrangement;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7451 - 7455
反应条件
in dichloromethane; toluene T=0°C; 0.166667 h;
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 7 p. 1932 - 1935
反应条件
tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; triethylamine in toluene T=110°C; 16 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 27 p. 11132 - 11135
反应条件
1: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C 2: triethylamine; diphenyl phosphoryl azide / 80 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7451 - 7455
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C 3: triethylamine; diphenyl phosphoryl azide / 80 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7451 - 7455
参考文献
Justus Liebigs Annalen der Chemie, , vol. 562, p. 75,1114
