1-甲氧基-4-(苯硫基)-苯合成路线 (共 118 条)
反应条件
1: C6H5SAc With potassium tert-butylate
0.166667 h;
2: para-iodoanisole With copper(l) iodide; 1,10-phenanthroline
T=100°C; 24 h;
参考文献
Soria-Castro, Silvia M.; Penenory, Alicia B.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 467 - 475
反应条件
1: copper(II) oxide / dimethyl sulfoxide / 4.5 h / 85 °C / Inert atmosphere
2: potassium hydroxide / dimethyl sulfoxide / 15 h / 85 °C / Inert atmosphere
View Scheme
参考文献
Akkilagunta, Vijay Kumar; Kakulapati, Rama Rao
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6819 - 6824
反应条件
pyridine; quinoline
T=200 - 210°C;
参考文献
Adams et al.
Croatica Chemica Acta, 1957 , vol. 29, p. 277,284, 285
Org. Synth. Coll., Vol V <1973> 107, 109
反应条件
pyridine; quinoline
T=200 - 210°C;
参考文献
Adams et al.
Croatica Chemica Acta, 1957 , vol. 29, p. 277,284, 285
Org. Synth. Coll., Vol V <1973> 107, 109
反应条件
sulfuric acid; trifluoroacetic acid
T=25°C; 0.5 h;
参考文献
Takeuchi, Hiroshi; Oya, Hiromo; Yanase, Takehiro; Itou, Katsutaka; Adachi, Taki; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 4 p. 827 - 834
反应条件
in toluene
T=20°C; 0.166667 h; Inert atmosphereSealed tube;
参考文献
Cheng, Jun-Hao; Ramesh, Chintakunta; Kao, Hsin-Lun; Wang, Yu-Jen; Chan, Chien-Ching; Lee, Chin-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10369 - 10374
反应条件
in tetrahydrofuran; dichloromethane
T=24°C; Inert atmosphere;
参考文献
Yonova, Ivelina M.; Osborne, Charlotte A.; Morrissette, Naomi S.; Jarvo, Elizabeth R.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 1947 - 1953
反应条件
dimethyl sulfoxide; potassium hydroxide
T=130°C; 24 h; Inert atmosphere;
参考文献
Yuan, Yu; Thome, Isabelle; Kim, Seok Hwan; Chen, Duanteng; Beyer, Astrid; Bonnamour, Julien; Zuidema, Erik; Chang, Sukbok; Bolm, Carsten
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2892 - 2898
反应条件
dimethyl sulfoxide; potassium hydroxide
T=130°C; 24 h; Inert atmosphere;
参考文献
Yuan, Yu; Thome, Isabelle; Kim, Seok Hwan; Chen, Duanteng; Beyer, Astrid; Bonnamour, Julien; Zuidema, Erik; Chang, Sukbok; Bolm, Carsten
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2892 - 2898
反应条件
in acetonitrile-D3
T=45°C; Inert atmosphereDarkness; regioselective reaction;
参考文献
Wang, Bijia; Graskemper, Joseph W.; Qin, Linlin; DiMagno, Stephen G.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4079 - 4083