1-甲氧基-4-(苯硫基)-苯合成路线 （共 118 条）
反应条件
potassium tert-butylate; Josiphos SL-J009-1; bis(dibenzylideneacetone)-palladium(0) in toluene
T=110°C; 4 - 12 h; Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2007/64869 A2, 2007 ;
Location in patent: Page/Page column 17-18 ;
反应条件
[2,2']bipyridinyl; copper(l) iodide in water; dimethyl sulfoxide
T=100°C; 12 h;
参考文献
Taniguchi, Nobukazu
Synlett, 2006 , # 9 p. 1351 - 1354
反应条件
copper(l) iodide; trans-1,2-cyclohexanediol; potassium carbonate in isopropyl alcohol
T=120°C; Ullmann type coupling; 3 h; Microwave irradiation;
参考文献
Bagley, Mark C.; Davis, Terence; Dix, Matthew C.; Fusillo, Vincenzo; Pigeaux, Morgane; Rokicki, Michal J.; Kipling, David
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8336 - 8342
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; 1 h;
参考文献
Wang; Chen
Synthetic Communications, 2001 , vol. 31, # 8 p. 1227 - 1232
反应条件
1: para-iodoanisole With (R)-(+)-1,1'-binaphthyl-2,2'-diamine; copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide
T=105°C; Ullmann type reaction; 24 h; Inert atmosphere;
2: iodobenzene With potassium hydroxide in N,N-dimethyl-formamide
T=105°C; 24 h; Inert atmosphere;
参考文献
Prasad; Sekar, Govindasamy
Organic Letters, 2011 , vol. 13, # 5 p. 1008 - 1011
反应条件
bis-triphenylphosphine-palladium(II) chloride; pivalic acid potassium salt in N,N-dimethyl acetamide
T=140°C; 12 h; Reagent/catalyst;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
hydrogenchloride; potassium iodide in chloroform
T=0 - 5°C;
参考文献
Chasar, Dwight W.; Shockcor, John P.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 187 - 188
反应条件
[2,2']bipyridinyl; copper(l) iodide in water; dimethyl sulfoxide
T=100°C; 48 h;
参考文献
Taniguchi, Nobukazu
Synlett, 2006 , # 9 p. 1351 - 1354
反应条件
potassium hydroxide; tetrabutylammomium bromide; copper(l) iodide in water
T=80°C; 15 h;
参考文献
Rout, Laxmidhar; Saha, Prasenjit; Jammi, Suribabu; Punniyamurthy, Tharmalingam
European Journal of Organic Chemistry, 2008 , # 4 p. 640 - 643
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
