1-甲氧基-4-(苯硫基)-苯合成路线 （共 118 条）
反应条件
potassium carbonate in acetonitrile
T=100°C; 0.5 h; Microwave irradiation;
参考文献
Gonzalez-Arellano, Camino; Luque, Rafael; MacQuarrie, Duncan J.
Chemical Communications, 2009 , # 11 p. 1410 - 1412
反应条件
1: 3,4,5-trimethoxyphenylboronic acid With potassium ethylxanthate; copper(l) chloride in methanol
3 h; Inert atmosphereReflux;
2: (4-methoxyphenyl)-boronic acid With potassium hydroxide in methanol
5 h; Inert atmosphereReflux;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Synlett, 2011 , # 20 art. no. W18411ST, p. 3041 - 3045
反应条件
copper(l) iodide; zinc diacetate
T=140°C; 24 h; Reagent/catalyst; chemoselective reaction;
参考文献
Joseph, P.J. Amal; Priyadarshini; Kantam, M. Lakshmi; Sreedhar
Tetrahedron, 2013 , vol. 69, # 38 p. 8276 - 8283
反应条件
trifluoroacetic acid in 1,4-dioxane
T=110°C; 15 h;
参考文献
Wagner, Anna M.; Sanford, Melanie S.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2263 - 2267
反应条件
n-Bu4N+CN- in dimethyl sulfoxide
T=25°C; 1 h; Irradiation;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'erba, Carlo
Tetrahedron, 1987 , vol. 43, # 20 p. 4625 - 4634
反应条件
N,N-dicyclohexylmethylamine; sodium acetate; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in ethylene glycol dimethyl ether
T=85°C; 18 h; Reagent/catalystSolvent; Overall yield = 82 percent; chemoselective reaction;
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
silver hexafluoroantimonate; antimony(V) pentachloride in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Mukaiyama, Teruaki; Suzuki, Kaoru
Chemistry Letters, 1993 , # 1 p. 1 - 4
反应条件
1: Na / diethyl ether / 24 h
2: 80 percent / o-phenylene-bis<diphenylphosphino>-nickel(II) bromide / ethane-1,2-diol / 24 h / 200 °C
View Scheme
参考文献
Cristau, H. J.; Chabaud, B.; Chene, A.; Christol, H.
Synthesis, 1981 , # 11 p. 892 - 894
反应条件
1: carbon tetrachloride; chlorine
2: diethyl ether
3: alkali
View Scheme
参考文献
Lecher
Chemische Berichte, 1925 , vol. 58, p. 415
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=120°C; 20 h;
参考文献
Kosugi, Masanori; Ogata, Toshimi; Terada, Masahiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3657 - 3658
