1-甲氧基-4-(苯硫基)-苯合成路线 （共 118 条）
反应条件
1: 90 percent / AlCl3 / CH2Cl2
2: 100 percent / phenol, HCl / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Chasar, Dwight W.; Pratt, Timothy M.; Shockcor, J. P.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 183 - 186
反应条件
1: 90 percent / AlCl3 / CH2Cl2
2: 100 percent / phenol, HCl / CH2Cl2 / 0 - 25 °C
View Scheme
参考文献
Chasar, Dwight W.; Pratt, Timothy M.; Shockcor, J. P.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 183 - 186
反应条件
2: methanolic sodium methylate
View Scheme
参考文献
Hinsberg
Chemische Berichte, 1903 , vol. 36, p. 112
Full Text Show Details
Hoechster Farbw.
Patent: DE147634 ;
反应条件
1.1: sulfuryl dichloride; triethylamine / dichloromethane / 0 - 20 °C
1.2: 1 h / 0 - 20 °C
2.1: palladium diacetate; trifluoroacetic acid / 0.75 h / 20 °C
View Scheme
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
1.1: sulfuryl dichloride; triethylamine / dichloromethane / 0 - 20 °C
1.2: 1 h / 0 - 20 °C
2.1: palladium diacetate; trifluoroacetic acid / 0.75 h / 20 °C
3.1: pivalic acid potassium salt; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl acetamide / 12 h / 140 °C
View Scheme
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
参考文献
Hilbert; Johnson
Journal of the American Chemical Society, 1929 , vol. 51, p. 1533
反应条件
2: methanolic sodium methylate
View Scheme
参考文献
Hinsberg
Chemische Berichte, 1903 , vol. 36, p. 112
Full Text Show Details
Hoechster Farbw.
Patent: DE147634 ;
反应条件
cesium fluoride in toluene
T=110°C; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Chemistry - A European Journal, 2010 , vol. 16, # 8 p. 2355 - 2359
反应条件
cesium fluoride in toluene
T=110°C; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Chemistry - A European Journal, 2010 , vol. 16, # 8 p. 2355 - 2359
反应条件
potassium hydroxide in dimethyl sulfoxide
T=85°C; 15 h; Inert atmosphere;
参考文献
Akkilagunta, Vijay Kumar; Kakulapati, Rama Rao
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6819 - 6824
