1-甲氧基-4-(苯硫基)-苯合成路线 （共 118 条）
反应条件
1: palladium diacetate; trifluoroacetic acid / 0.75 h / 20 °C
2: pivalic acid potassium salt; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl acetamide / 12 h / 140 °C
View Scheme
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
palladium diacetate; trifluoroacetic acid
T=20°C; 0.75 h; Overall yield = 89 percent;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
in dimethyl sulfoxide
T=25°C; 1 h; Irradiation;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'erba, Carlo
Tetrahedron, 1987 , vol. 43, # 20 p. 4625 - 4634
反应条件
1: copper(l) iodide; Na2S*9H2O; sulfur / N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere
2: iron; potassium carbonate / dimethyl sulfoxide; N,N-dimethyl-formamide / 18 h / 120 °C / Inert atmosphere
View Scheme
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
tert.-butylnitrite; C29H23N6Ru2(2+)*2Cl(1-)*6H2O; toluene-4-sulfonic acid in acetonitrile
T=25°C; 1 h; Reagent/catalyst;
参考文献
Wang, Xiao; Cuny, Gregory D.; Noel, Timothy
Angewandte Chemie - International Edition, 2013 , vol. 52, # 30 p. 7860 - 7864
Angew. Chem., 2013 , vol. 125, # 30 p. 8014 - 8018,5
参考文献
Hinsberg
Chemische Berichte, 1903 , vol. 36, p. 112
Full Text Show Details
Hilbert; Johnson
Journal of the American Chemical Society, 1929 , vol. 51, p. 1533
反应条件
1: N-chloro-succinimide / toluene / 0.33 h / 20 °C / |Inert atmosphere; |Sealed tube
2: toluene / 0.17 h / 20 °C / |Inert atmosphere; |Sealed tube
View Scheme
参考文献
Cheng, Jun-Hao; Ramesh, Chintakunta; Kao, Hsin-Lun; Wang, Yu-Jen; Chan, Chien-Ching; Lee, Chin-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10369 - 10374
反应条件
C29H23N6Ru2(2+)*2Cl(1-)*6H2O; toluene-4-sulfonic acid; isopentyl nitrite in acetonitrile
T=25°C; 1 h;
参考文献
Wang, Xiao; Cuny, Gregory D.; Noel, Timothy
Angewandte Chemie - International Edition, 2013 , vol. 52, # 30 p. 7860 - 7864
Angew. Chem., 2013 , vol. 125, # 30 p. 8014 - 8018,5
反应条件
1.1: 69 percent / benzene / Heating
2.1: Na / diethyl ether / Heating
2.2: 2.3 percent / acetonitrile / 20 °C
View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide
T=130°C; 48 h; Inert atmosphere;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
