1,5-二甲基-2-吡咯甲腈合成路线 （共 8 条）
反应条件
hydrogenchloride; n-butyllithium in tetrahydrofuran; hexane T=-100°C; 0.25 h;
参考文献
New Journal of Chemistry, , vol. 27, # 10 p. 1425 - 1432
反应条件
trichlorophosphate T=20°C; 3 h;
参考文献
Ryabukhin, Sergey V.; Plaskon, Andrey S.; Volochnyuk, Dmitriy M.; Tolmachev, Andrey A.
Synthesis, 2006 , # 21 p. 3715 - 3726
反应条件
((n-Bu)4N)2S2O8; lithium bromide in acetonitrile T=25°C; 8 h;
参考文献
Park, Min Young; Yang, Seung Gak; Jadhav, Vidyadhar; Kim, Yong Hae
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4887 - 4890
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Min, Young Park; Seung, Gak Yang; Kim, Yong Hae
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 5-6 p. 1235 - 1240
反应条件
bromine; acetic acid T=20°C; 24 h; Title compound not separated from byproducts.;
参考文献
Li, Xue; Liu, Gang; Zheng, Chunhong; Fan, Congbin; Pu, Shouzhi
Tetrahedron, 2014 , vol. 70, # 26 p. 3971 - 3975
参考文献
Yoshida, Seigo; Kubo, Hiroaki; Saika, Tetsuyuki; Katsumura, Shigeo
Chemistry Letters, 1996 , # 2 p. 139 - 140
反应条件
in dichloromethane; water
参考文献
Ethyl Corporation
Patent: US4187230 A1, 1980 ;
反应条件
lithium aluminium tetrahydride in diethyl ether 10 h; Ambient temperature;
参考文献
Tseng, Pen-Wen; Chou, Chin-Hsing
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 5 p. 579 - 584
反应条件
1: 90 percent / LiAlH4 / diethyl ether / 10 h / Ambient temperature
2: 91 percent / Et3N / diethyl ether / 10 h / Heating
3: 560 °C / 0 Torr
View Scheme
参考文献
Tseng, Pen-Wen; Chou, Chin-Hsing
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 5 p. 579 - 584
