2,2-二甲基-3-戊酮合成路线 (共 63 条)
反应条件
in benzene React. of starting compounds at 25°C for 24h.;
参考文献
Journal of the American Chemical Society, , vol. 111, # 3 p. 938 - 949
反应条件
aluminium trichloride in dichloromethane 18 h; Heating;
参考文献
Tetrahedron, , vol. 59, # 34 p. 6393 - 6402
反应条件
hydrogenchloride in water 0.5 h; Ambient temperature; Yield given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
1: 1.) Mg 2: pyridinium chlorochromate / CH2Cl2 View Scheme
参考文献
Organic Mass Spectrometry, , vol. 28, # 10 p. 1189 - 1196
反应条件
1: 100 percent / n-butyllithium / tetrahydrofuran; diethyl ether / 0.25 h / -70 °C 2: tetrahydrofuran / 0.5 h / -65 °C 3: 1.2 N HCl / H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
1: tetrahydrofuran / 0.5 h / -65 °C 2: 1.2 N HCl / H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
1: 1.) Br2 2.) NEt3 / 1.) ether, -60 deg C, 0.5 h, then 0 deg C; 2.) ether, -20 deg C 2: 100 percent / n-butyllithium / tetrahydrofuran; diethyl ether / 0.25 h / -70 °C 3: tetrahydrofuran / 0.5 h / -65 °C 4: 1.2 N HCl / H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
ammonia; sodium Umsetzen des Reaktionsprodukts mit Aethylbromid;
参考文献
Journal of Organic Chemistry, , vol. 5, p. 362,375
反应条件
diethyl ether T=-70°C;
参考文献
Journal of the Chemical Society, , p. 2705
反应条件
T=364.9 - 453.9°C; P=8 Torr; pyrolysis; Further byproducts given;
参考文献
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, , vol. 79, p. 2179 - 2184