2-苄基-3-氧代-3-苯基丙酸乙酯合成路线 (共 23 条)
反应条件
potassium carbonate; sodium iodide
T=65°C; 60 h;
参考文献
Queignec, Rene; Kirschleger, Bernard; Lambert, Francois; Aboutaj, Mohammed
Synthetic Communications, 1988 , vol. 18, # 11 p. 1213 - 1224
反应条件
[5-Cl-2-{(4-Cl-phenyl)-[(E)-HO-imino]methyl}phenyl-PdCl]2; tetrabutylammomium bromide; potassium carbonate in N,N-dimethyl-formamide
T=130°C; Heck reaction; 3 h;
参考文献
Ferreira, Bruno R.V.; Pirovani, Rodrigo V.; Souza-Filho, Luis G.; Coelho, Fernando
Tetrahedron, 2009 , vol. 65, # 36 p. 7712 - 7717
反应条件
titanium tetrachloride; triethylamine in acetonitrile
0.25 h; Heating;
参考文献
Taber, Douglass F.; Sheth, Ritesh B.; Joshi, Pramod V.
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2851 - 2854
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=60°C; 5 h; Inert atmosphere;
参考文献
He, Zhiheng; Li, Huanrong; Li, Zhiping
Journal of Organic Chemistry, 2010 , vol. 75, # 13 p. 4636 - 4639
反应条件
hantzsch ester in water
T=100°C; 24 h; Green chemistry; chemoselective reaction;
参考文献
He, Qi; Xu, Zhihong; Jiang, Dehong; Ai, Wensi; Shi, Ronghua; Qian, Shan; Wang, Zhouyu
RSC Advances, 2014 , vol. 4, # 17 p. 8671 - 8674
反应条件
tetrabutylammomium bromide; potassium acetate; palladium diacetate in acetonitrile
Heck reaction; 24 h; Heating;
参考文献
Kim, Jeong Mi; Kim, Ko Hoon; Kim, Taek Hyeon; Kim, Jae Nyoung
Tetrahedron Letters, 2008 , vol. 49, # 20 p. 3248 - 3251
反应条件
triphenylmethyllithium
1) THF; Yield given. Multistep reaction;
参考文献
Cohen, B. J.; Kraus, M. A.; Patchornik, A.
Journal of the American Chemical Society, 1981 , vol. 103, # 25 p. 7620 - 7629
反应条件
1.) 80 deg C, 4 h, 2.) 110 deg C, 2 h, 3.) 130 deg C, 5 h;
参考文献
Vartanyan, S. A.; Vartanyan, R. S.; Karamyan, S. A.; Avetyan, L. O.; Apoyan, N. A.; Melkonyan, Zh. S.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 7 p. 470 - 473
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 7 p. 821 - 825
反应条件
[bmim]Br; 1,8-diazabicyclo[5.4.0]undec-7-ene
T=25°C; 2 h;
参考文献
Ramachary, Dhevalapally B.; Narayana, Vidadala V.; Ramakumar, Kinthada
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2704 - 2709
反应条件
pyridine; hydroxylamine hydrochloride in ethanol
T=60°C; 18 h;
参考文献
Too, Pei Chui; Wang, Yi-Feng; Chiba, Shunsuke
Organic Letters, 2010 , vol. 12, # 24 p. 5688 - 5691