5,6-二氯-2,3-二氰基吡嗪合成路线 (共 10 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide in 1,4-dioxane T=100°C; 5 h;
参考文献
Suzuki, Toshinobu; Nagae, Yasushi; Mitsuhashi, Keiryo
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1419 - 1421
参考文献
US8742107 B1, ;
Page/Page column ;
反应条件
1: 2: With thionyl chloride
参考文献
Bures, Filip; Cermakova, Hana; Kulhanek, Jiri; Ludwig, Miroslav; Kuznik, Wojciech; Kityk, Iwan V.; Mikysek, Tomas; Ruzicka, Ales
European Journal of Organic Chemistry, 2012 , # 3 p. 529 - 538
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate Suzuki coupling;
参考文献
Ali, Hasrat; Van Lier, Johan E.
Tetrahedron Letters, 2012 , vol. 53, # 36 p. 4824 - 4827
反应条件
ammonia in tetrahydrofuran Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 34, # 2 p. 653 - 657
反应条件
in tetrahydrofuran 6 h; Heating;
参考文献
Musil, Zbynek; Zimcik, Petr; Miletin, Miroslav; Kopecky, Kamil; Lenco, Juraj
European Journal of Organic Chemistry, 2007 , # 27 p. 4535 - 4542
反应条件
hydrogenchloride in tetrahydrofuran; water
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4054655 A1, 1977 ;
反应条件
pyridine in n-butyl chloride; 1,2-dichloro-ethane
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4113724 A1, 1978 ;
反应条件
cadmium(II) perchlorate in ethanol; water
T=110°C; 72 h;
参考文献
Liu, Cai-Ming; Zhang, De-Qing; Qin, An-Jun; Ye, Chen; Hu, Huai-Ming; Zhu, Dao-Ben
European Journal of Inorganic Chemistry, 2002 , # 7 p. 1595 - 1598
反应条件
SS-Phos; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in water; acetonitrile
Suzuki coupling;
参考文献
Ali, Hasrat; Van Lier, Johan E.
Tetrahedron Letters, 2012 , vol. 53, # 36 p. 4824 - 4827