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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56419-18-2
合成路线
（共 11 条）
204591-33-3
→
反应条件
56419-18-2
反应条件
hydrogenchloride in methanol 2 h; Heating;
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Fujii, Kenichi; Tsukayama, Masao; Ohtsuru, Yoshizumi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 222 - 230
204590-96-5
→
反应条件
56419-18-2
反应条件
1: thallium (III) nitrate * 3H2O / methanol; CHCl3 / 20 h / 30 °C 2: H2 / 10percent Pd/C / methanol 3: 10percent aq. HCl / methanol / 2 h / Heating 4: 100 percent / pyridine 5: 91 percent / AlBr3 / acetonitrile / 0.67 h / 20 °C 6: 98 percent / 16percent aq. HCl / methanol / 2 h / Heating View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Fujii, Kenichi; Tsukayama, Masao; Ohtsuru, Yoshizumi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 222 - 230
204591-06-0
→
反应条件
56419-18-2
反应条件
1: H2 / 10percent Pd/C / methanol 2: 10percent aq. HCl / methanol / 2 h / Heating 3: 100 percent / pyridine 4: 91 percent / AlBr3 / acetonitrile / 0.67 h / 20 °C 5: 98 percent / 16percent aq. HCl / methanol / 2 h / Heating View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Fujii, Kenichi; Tsukayama, Masao; Ohtsuru, Yoshizumi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 222 - 230
64640-61-5
→
反应条件
56419-18-2
反应条件
aluminium trichloride in acetonitrile 3 h; Heating;
参考文献
Siiaw, S.C.; Gupta, Aniu Kumari; Kumar, Rajesh
Journal of the Indian Chemical Society, 1991 , vol. 68, # 11 p. 615 - 616
204591-16-2
→
反应条件
56419-18-2
反应条件
1: 10percent aq. HCl / methanol / 2 h / Heating 2: 100 percent / pyridine 3: 91 percent / AlBr3 / acetonitrile / 0.67 h / 20 °C 4: 98 percent / 16percent aq. HCl / methanol / 2 h / Heating View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Fujii, Kenichi; Tsukayama, Masao; Ohtsuru, Yoshizumi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 222 - 230
204591-51-5
→
反应条件
56419-18-2
反应条件
1: 91 percent / AlBr3 / acetonitrile / 0.67 h / 20 °C 2: 98 percent / 16percent aq. HCl / methanol / 2 h / Heating View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Fujii, Kenichi; Tsukayama, Masao; Ohtsuru, Yoshizumi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 222 - 230
6274-74-4
→
反应条件
56419-18-2
反应条件
1: zinc chloride, HCl / diethyl ether / 4 h / 0 °C 2: Na / Ambient temperature 3: aluminium chloride / acetonitrile / 3 h / Heating View Scheme
参考文献
Siiaw, S.C.; Gupta, Aniu Kumari; Kumar, Rajesh
Journal of the Indian Chemical Society, 1991 , vol. 68, # 11 p. 615 - 616
64640-60-4
→
反应条件
56419-18-2
反应条件
1: Na / Ambient temperature 2: aluminium chloride / acetonitrile / 3 h / Heating View Scheme
参考文献
Siiaw, S.C.; Gupta, Aniu Kumari; Kumar, Rajesh
Journal of the Indian Chemical Society, 1991 , vol. 68, # 11 p. 615 - 616
1699-39-4
(3-苄氧基-4-甲氧基苯基)-乙腈
→
反应条件
56419-18-2
反应条件
1: zinc chloride, HCl / diethyl ether / 4 h / 0 °C 2: Na / Ambient temperature 3: aluminium chloride / acetonitrile / 3 h / Heating View Scheme
参考文献
Siiaw, S.C.; Gupta, Aniu Kumari; Kumar, Rajesh
Journal of the Indian Chemical Society, 1991 , vol. 68, # 11 p. 615 - 616
38836-54-3
→
反应条件
56419-18-2
反应条件
1: acetic anhydride / 0.08 h 2: zinc chloride, HCl / diethyl ether / 4 h / 0 °C 3: Na / Ambient temperature 4: aluminium chloride / acetonitrile / 3 h / Heating View Scheme
参考文献
Siiaw, S.C.; Gupta, Aniu Kumari; Kumar, Rajesh
Journal of the Indian Chemical Society, 1991 , vol. 68, # 11 p. 615 - 616
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