magnesium in diethyl ether
(Ar); mixt. of (CH2)5Br2 and GeCl4 was added dropwise to Mg in Et2O; several drops of Br(CH2)3Br was added; heated for 0.5 h; quenched with H2O and 5percent HCl; extd. (Et2O); dried (CaCl2); distd. (vac.);
参考文献
Amosova, Svetlana V.; Penzik, Maxim V.; Martynov, Alexander V.; Makhaeva, Nataliya A.; Yarosh, Nina O.; Voronkov, Mikhail G.
Journal of Organometallic Chemistry, 2008 , vol. 693, # 21-22 p. 3346 - 3350
