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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56461-02-0
合成路线
（共 10 条）
113388-94-6
→
反应条件
56461-02-0
+
113388-70-8
+
113388-71-9
反应条件
dihydrogen peroxide; O,O'-dinitrodiphenyl diselenide in dichloromethane 23 h; Ambient temperature;
参考文献
Syper, Ludwik
Tetrahedron, 1987 , vol. 43, # 12 p. 2853 - 2872
108-86-1
溴代苯
→
反应条件
56461-02-0
反应条件
1: 1.) Mg 2: sodium dichromate, conc. H2SO4, sodium benzosulfonate / H2O / 4.5 h / 50 - 55 °C View Scheme
参考文献
Nowicki, Ryszard
Polish Journal of Chemistry, 1987 , vol. 61, # 1-3 p. 73 - 76
529-34-0
1-四氢萘酮
→
反应条件
56461-02-0
反应条件
1: 1.) Mg 2: sodium dichromate, conc. H2SO4, sodium benzosulfonate / H2O / 4.5 h / 50 - 55 °C View Scheme
参考文献
Nowicki, Ryszard
Polish Journal of Chemistry, 1987 , vol. 61, # 1-3 p. 73 - 76
1961-97-3
3-苯基-1H-茚
→
反应条件
56461-02-0
反应条件
1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux 2: sodium periodate 4: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
36374-47-7
→
反应条件
56461-02-0
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux 3: sodium periodate 5: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
83-33-0
1-茚酮
→
反应条件
56461-02-0
反应条件
1: tetrahydrofuran / 20 °C 2: boron trifluoride diethyl etherate / dichloromethane / 20 °C 3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux 4: sodium periodate 6: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
100-58-3
溴化苯基镁
→
反应条件
56461-02-0
反应条件
1: tetrahydrofuran / 20 °C 2: boron trifluoride diethyl etherate / dichloromethane / 20 °C 3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux 4: sodium periodate 6: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
1224455-17-7
→
反应条件
56461-02-0
反应条件
1: sodium periodate 3: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
58668-70-5
→
反应条件
56461-02-0
反应条件
2: Jone's reagent View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
56461-02-0
→
反应条件
56461-08-6
反应条件
1: thionyl chloride 2: AlCl3, aluminium chloride View Scheme
参考文献
Chang, Meng-Yang; Lee, Nien-Chia
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 306 - 308
