甲基2-甲氧基-1-吡咯烷羧酸酯合成路线 （共 27 条）
反应条件
tetrachlorosilane; titanium tetrachloride in dichloromethane
T=-78 - 20°C; Mannich-type reaction; Inert atmosphere;
参考文献
Kamogawa, Satoshi; Ikeda, Takashi; Kuriyama, Masami; Matsumura, Yoshihiro; Onomura, Osamu
Heterocycles, 2010 , vol. 82, # 1 p. 325 - 332
反应条件
Nafion H in dichloromethane
96 h; Ambient temperature;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Tsubata, Kenji
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1172 - 1176
反应条件
hydrogenchloride; titanium tetrachloride in dichloromethane
T=-5 - 5°C; 3 h; further Lewis acids (BF3*(OC2H5)3);
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Tsubata, Kenji
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1172 - 1176
反应条件
titanium tetrachloride in dichloromethane
1) -70 deg C, 2) -20 deg C, 2 h;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Uchida, Kenshi; Tsubata, Kenji; Makino, Atsushi
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 300 - 304
反应条件
titanium tetrachloride in dichloromethane
T=-30 - 0°C;
参考文献
Pousset, Cyrille; Callens, Roland; Haddad, Mansour; Larcheveque, Marc
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3407 - 3412
反应条件
1: 92 percent / TiCl4 / CH2Cl2 / 1 h / 0 °C
2: 75 percent / tetraethylammonium p-toluenesulfonate / dimethylformamide / carbon rod anode; zinc cathode; 3.0 F/mol
View Scheme
参考文献
Shono, Tatsuya; Terauchi, Jun; Kitayama, Kenji; Takeshima, Yo-Ichiro; Masumura, Yoshihiro
Tetrahedron, 1992 , vol. 48, # 38 p. 8253 - 8262
反应条件
zinc(II) chloride in xylene
Heating;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kanazawa, Takenobu
Tetrahedron Letters, 1983 , vol. 24, # 12 p. 1259 - 1262
