反应条件
1: 1.) trimethylchlorosilane, NaI / 1.) MeCN, 50 deg C, 4 h
2: 4-(dimethylamino)pyridine / CH2Cl2 / 0.5 h / 0 °C
3: K2CO3 / methanol / 1.5 h / 23 °C
View Scheme
参考文献
Corey, E. J.; Shimoji, Katsuichi
Journal of the American Chemical Society, 1983 , vol. 105, # 6 p. 1662 - 1664