1,4,7-三氮杂环壬烷-N,N',N''-三乙酸合成路线 （共 4 条）
参考文献
CONCAT LP, a California Limited Partnership
Patent: US2005/112066 A1, 2005 ;
Location in patent: Page/Page column 26 ;
反应条件
lithium hydroxide hydrate in water
T=45°C; pH=10; Reflux;
参考文献
Majkowska-Pilip; Bilewicz
Journal of Inorganic Biochemistry, 2011 , vol. 105, # 2 p. 313 - 320
反应条件
sodium hydroxide in water
3 h;
参考文献
De Vos, Dirk E.; Bein, Thomas
Journal of Organometallic Chemistry, 1996 , vol. 520, # 1-2 p. 195 - 200
反应条件
1: sodium hydroxide / water / pH 12
2: sodium carbonate / 24 h / 50 °C / |Inert atmosphere
3: trifluoroacetic acid / 24 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Maheshwari, Vidhi; Dearling, Jason L.J.; Treves, S. Ted; Packard, Alan B.
Inorganica Chimica Acta, 2012 , vol. 393, p. 318 - 323
