3-甲基-3-戊烯-2-酮合成路线 （共 23 条）
反应条件
hydrogen bromide T=180°C;
参考文献
Hoffmann, H. M. R.; Vathke-Ernst, Heidrun
Chemische Berichte, 1981 , vol. 114, # 8 p. 2898 - 2906
反应条件
Nafion-H in tetrachloromethane 16 h; Heating;
参考文献
Olah, George A.; Fung, Alexander P.
Synthesis, 1981 , # 6 p. 473 - 474
反应条件
in diethyl ether T=-78°C; 10 h;
参考文献
Richey, Herman G.; Bension, Rouvain M.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5036 - 5042
反应条件
bei der Einwirkung von γ-Strahlung;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1117,1119
反应条件
Ru/Al; hydrogen T=150°C; P=22502.3 Torr; 7 h; Large scale;
参考文献
International Flavors and Fragrances Inc.; Adell Gavalda, Juan; P.S. Narula, Anubhav; Collado Perez, Ana Maria
Patent: EP2708536 A1, 2014 ;
Location in patent: Paragraph 0019 ;
反应条件
cis-Ru(phen)2Cl2; potassium tert-butylate; hydrogen in butan-1-ol T=100°C; P=15301.5 Torr; Autoclave; chemoselective reaction;
参考文献
Deshmukh, Amit; Kinage, Anil; Kumar, Rajiv; Meijboom, Reinout
Polyhedron, 2010 , vol. 29, # 17 p. 3262 - 3268
反应条件
palladium on activated charcoal; hydrogen T=85°C; P=7500.75 Torr; 3.5 h; Large scale;
参考文献
International Flavors and Fragrances Inc.; Adell Gavalda, Juan; P.S. Narula, Anubhav; Collado Perez, Ana Maria
Patent: EP2708536 A1, 2014 ;
Location in patent: Paragraph 0013 ;
反应条件
1: 52 percent / hydrochloric acid / ethanol / 5 h / Heating 2: methylamine / H2O; ethanol / Ambient temperature View Scheme
参考文献
Casy, Alan F.; Ogungbamila, Francis O.; Rostron, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 749 - 754
参考文献
Corey,E.J.; Hegedus,L.S.
Journal of the American Chemical Society, 1969 , vol. 91, p. 4926 - 4928
反应条件
trichlorophosphate 1.) 30 min, room temperature, 2.) 4-4.5 h, boiling water-bath;
参考文献
Sreenivasulu, M.; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 494 - 495
