苯基(2-甲基-1-丙烯基)甲酮合成路线 (共 92 条)
反应条件
(i), (ii) (pyrolysis); Multistep reaction;
参考文献
Tolbert,L.M.
Journal of Organic Chemistry, 1979 , vol. 44, # 25 p. 4584 - 4588
反应条件
aluminium trichloride; cyclohexane in dichloromethane T=20°C; 3 h;
参考文献
Koltunov; Repinskaya; Borodkin
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 11 p. 1534 - 1541
反应条件
air; ammonium cerium(IV) nitrate in ethanol T=20°C; 0.666667 h;
参考文献
Tetrahedron, , vol. 63, # 8 p. 1863 - 1871
反应条件
1: 2) H2 / 2) Ni 2: 74 percent / HBF4*Et2O / CH2Cl2 / 2 h / Ambient temperature 3: 75 percent / MCPBA, KF / N,N-dimethyl-acetamide / 6 h / 60 °C View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
反应条件
lithium iodide in diethyl ether T=25°C; stopped-flow ultraviolet spectroscopy; kinetics and mechanism of the conjugate addition of lithium dimethylcuprate to α,β-unsaturated ketones, substituent effect;
参考文献
House,H.O. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 19 p. 3067 - 3076
反应条件
HUSY-zeolite in tetrachloromethane T=130°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 46, # 48 p. 8391 - 9394
反应条件
triazole-Au in methanol; water
T=60°C; Meyer-Schuster rearrangement; 3 h;
参考文献
Wang, Dawei; Zhang, Yanwei; Harris, Alexandria; Gautam, Lekh Nath S.; Chen, Yunfeng; Shi, Xiaodong
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2584 - 2588
反应条件
[Ir(COD)(SnCl3)Cl(μ-Cl)]2; 1,3-diphenyl-1,3-propanedione in 1,2-dichloro-ethane
T=80°C; 0.583333 h; Inert atmosphere;
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2011 , vol. 67, # 25 p. 4569 - 4577
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; 3 h;
参考文献
Mugishima, Takao; Tsuda, Masashi; Kasai, Yuu; Ishiyama, Haruaki; Fukushi, Eri; Kawabata, Jun; Watanabe, Masayuki; Akao, Kenichi; Kobayashi, Jun'ichi
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9430 - 9435
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene
T=90°C;
参考文献
Liu, Lei; Montgomery, John
Journal of the American Chemical Society, 2006 , vol. 128, # 16 p. 5348 - 5349