苯基(2-甲基-1-丙烯基)甲酮合成路线 （共 92 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
1 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane
T=-20°C; 1 h; Irradiation;
参考文献
Russell, Glen A.; Mudryk, Boguslaw; Ros, Francisco; Jawdosiuk, Mikolaj
Tetrahedron, 1982 , vol. 38, # 8 p. 1059 - 1068
反应条件
potassium phosphate; bis-triphenylphosphine-palladium(II) chloride in toluene
T=80°C; 4 h;
参考文献
Urawa, Yoshio; Nishiura, Katsutoshi; Souda, Shigeru; Ogura, Katsuyuki
Synthesis, 2003 , # 18 p. 2882 - 2885
反应条件
1: LDA / tetrahydrofuran; hexane / -78 - 0 °C
2: 86 percent / 10percent NaOH / tetrabutylammonium hydrogen sulfate / H2O; CH2Cl2
View Scheme
参考文献
Hendrickson, James B.; Boudreaux, Gerald J.; Palumbo, Paul S.
Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2358 - 2366
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran; hexane
T=-20°C; 1 h; Irradiation;
参考文献
Russell, Glen A.; Mudryk, Boguslaw; Jawdosiuk, Mikolaj
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4610 - 4611
反应条件
dodecacarbonyltetrarhodium(0) in benzene
T=100°C; 15 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tris(4-methylphenyl)-phosphine in toluene
T=150°C; 12 h; Inert atmosphere;
参考文献
Rodriguez, Nuria; Manjolinho, Filipe; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemistry - A European Journal, 2011 , vol. 17, # 49 p. 13688 - 13691
反应条件
aluminium trichloride
T=0 - 40°C; P=150 Torr;
参考文献
Smith; Engelhardt
Journal of the American Chemical Society, 1949 , vol. 71, p. 2671,2674
反应条件
in tetrahydrofuran
T=-78°C; 0.75 h;
参考文献
Bates, Robert B.; Gordon, Bernard; Keller, Philip C.; Rund, John V.; Mills, Nancy S.,
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 168 - 169
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
Ambient temperature;
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Chemistry Letters, 1995 , # 11 p. 987 - 988
