苯基(2-甲基-1-丙烯基)甲酮合成路线 （共 92 条）
反应条件
hydrogenchloride in water; acetone
5 h; Heating;
参考文献
Lui, Kon-Hung; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 457 - 468
反应条件
potassium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=80°C; Yield given. Yields of byproduct given;
参考文献
Snowden, Roger L.; Linder, Simon M.; Muller, Bernard L.; Schulte, Karl H.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1858 - 1878
反应条件
aluminium trichloride in dichloromethane
12 h; Ambient temperature;
参考文献
Bonini, Bianca F.; Comes Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Ricci, Alfredo
Tetrahedron, 1997 , vol. 53, # 23 p. 7897 - 7910
反应条件
1: thionyl chloride
2: AlCl3 / 5 h / 0 °C
View Scheme
参考文献
Wagner, Peter J.; Thomas, Michael J.; Puchalski, Allen E.
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7739 - 7744
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
2 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
mercury dichloride; zinc in diethyl ether; ethyl acetate
T=55 - 60°C; 0.5 h;
参考文献
Shchepin, V. V.; Gladkova, G. E.; Russkikh, N. Yu.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 6.1 p. 902 - 907
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 6 p. 1156 - 1162
反应条件
1: 1.) TiCl4 / 1) CH2Cl2, -78 deg C, 1 min; 2) CH2Cl2, -78 deg C, 3 h
2: Et3N / CH2Cl2 / 1) 0 deg C, 10 min; 2) 0 deg C --> rt, 1 h
3: 70 percent / DBU / benzene / 1.5 h / Ambient temperature
View Scheme
参考文献
Otera, Junzo; Fujita, Yukihiro; Sakuta, Nobuyuki; Fujita, Morifumi; Fukuzumi, Shunichi
Journal of Organic Chemistry, 1996 , vol. 61, # 9 p. 2951 - 2962
参考文献
Gaudemar,M.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1974 , vol. 278, p. 533 - 535
反应条件
aluminium trichloride in dichloromethane
12 h; Ambient temperature;
参考文献
Bonini, Bianca F.; Comes Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Ricci, Alfredo
Tetrahedron, 1997 , vol. 53, # 23 p. 7897 - 7910
反应条件
1.1: magnesium / tetrahydrofuran / 1 h / Heating
1.2: 99 percent / tetrahydrofuran / 1 h
2.1: 81 percent / manganese(IV) oxide / CH2Cl2 / 3 h / 20 °C
View Scheme
参考文献
Mugishima, Takao; Tsuda, Masashi; Kasai, Yuu; Ishiyama, Haruaki; Fukushi, Eri; Kawabata, Jun; Watanabe, Masayuki; Akao, Kenichi; Kobayashi, Jun'ichi
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9430 - 9435
