苯基(2-甲基-1-丙烯基)甲酮合成路线 (共 92 条)
反应条件
sodium hydroxide
T=70°C; 2 h; Sealed ampule;
参考文献
Zenkevich; Ukolov
Russian Journal of General Chemistry, 2011 , vol. 81, # 9 p. 1818 - 1828
参考文献
House,H.O. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 19 p. 3067 - 3076
反应条件
1-ethyl-piperidine; dichloro bis(acetonitrile) palladium(II); tin(II) trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine
1.) methylene chloride, 0 deg C, 15 min; 2.) methylene chloride, RT; Yield given. Multistep reaction;
参考文献
Mukaiyama, Teruaki; Ohshima, Masahiro; Nakatsuka, Takashi
Chemistry Letters, 1983 , p. 1207 - 1210
反应条件
anhydrous cadmium carbonate; water; mercury dichloride
Yields of byproduct given;
参考文献
Donaldson; Hossain
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4107 - 4110
反应条件
in benzene
3.5 h; Irradiation;
参考文献
Grant, Richard D.; Pinhey, John T.; Rizzardo, Ezio; Smith, Geoffrey C.
Australian Journal of Chemistry, 1985 , vol. 38, # 10 p. 1505 - 1519
反应条件
ethanol; potassium iodide
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
titanium tetrachloride; triethylamine; trifluoroacetic anhydride
Yield given. Multistep reaction;
参考文献
Bouhlel; Hassine
Synthetic Communications, 1992 , vol. 22, # 15 p. 2183 - 2186
反应条件
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
Yield given. Yields of byproduct given;
参考文献
Donaldson; Hossain
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4107 - 4110
反应条件
1: AlCl3
2: KI; alcohol
View Scheme
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
1: phosphorus oxychloride; phosphorus pentachloride / bei moeglichst tiefer Temperatur
2: AlCl3
3: KI; alcohol
View Scheme
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393