(E)-氰基(羟基亚胺)乙酸乙酯合成路线 （共 7 条）
反应条件
sodium dithionite; sodium hydrogencarbonate in water T=20°C; 2.08333 h;
参考文献
Buettelmann, Bernd; Ceccarelli, Simona Maria; Jaeschke, Georg; Kolczewski, Sabine; Porter, Richard Hugh Philip; Vieira, Eric
Patent: US2006/160857 A1, 2006 ;
Location in patent: Page/Page column 37 ;
US 20060160857 A1
参考文献
Lonza Ltd.
Patent: US5003099 A1, 1991 ;
反应条件
1: sodium hydrogencarbonate; sodium dithionite / water / 2 h / 35 °C 2: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 20 °C 3: hydrogenchloride / 1,4-dioxane / 10 h / Reflux View Scheme
参考文献
Wang, Xiaojing; Ebens, JR., Allen J.
Patent: US2011/59961 A1, 2011 ;
US 20110059961 A1
反应条件
1: sodium hydrogencarbonate; sodium dithionite / water / 2 h / 35 °C 2: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 20 °C 3: Lawesson's reagent / pyridine / 15 h / Reflux View Scheme
参考文献
GENENTECH, INC.; Hodges, Alastair James; Matteucci, Mizio; Sharpe, Andrew; Sun, Minghua; Wang, Xiaojing; Tsui, Vickie H.
Patent: US2013/79321 A1, 2013 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 5 h;
参考文献
Kai, Hiroyuki; Matsumoto, Hiroshi; Hattori, Naohiko; Takase, Akira; Fujiwara, Tamio; Sugimoto, Hirohiko
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 15 p. 1997 - 2000
反应条件
potassium carbonate in acetone
Methylation; 2 h; Heating;
参考文献
Smith, Paul H.; Chamberlain, Keith; Sugars, Jane M.; Bromilow, Richard H.
Pesticide Science, 1995 , vol. 44, # 3 p. 219 - 224
参考文献
Mishchenko,A.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 121 - 128
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, p. 131 - 139
