1-(3,4-二甲氧基苯基)乙醇合成路线 （共 29 条）
参考文献
Rhodia Chimie
Patent: US6362378 B1, 2002 ;
Location in patent: Example 15 ;
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux 3: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux 3: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 4: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux 5: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry 6: 25 °C View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
1: 0.25 h / 120 °C / Microwave irradiation; Ionic liquid 2: dihydrogen peroxide / water / 72 h / 37 °C / Ionic liquid; Enzymatic reaction View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
chlorine dioxide in water T=25°C; pH=4;
参考文献
Svenson, Doug; Kadla, John F.; Chang, Hou-Min; Jameel, Hasan
Canadian Journal of Chemistry, 2002 , vol. 80, # 7 p. 761 - 766
反应条件
chlorine dioxide; sodium sulfate in water T=20 - 40°C; E(excit.); var. of pH, ionic strength; reaction in presence of chloride; Thermodynamic dataMechanismKinetics;
参考文献
Gunnarsson, N. Per-Ivar; Ljunggren, Sten C. Hj.
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 422 - 431
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux 3: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 4: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux 5: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 4 p. 781 - 787
反应条件
C6mim(1+)Br(1-) T=140°C; 0.2 h; Microwave irradiationCombinatorial reaction / High throughput screening (HTS); chemoselective reaction;
参考文献
Kumar, Rakesh; Sharma, Abhishek; Sharma, Naina; Kumar, Vinod; Sinha, Arun K.
European Journal of Organic Chemistry, 2008 , # 33 p. 5577 - 5582
反应条件
potassium dichromate; aluminium trichloride 0.05 h;
参考文献
Mohammadpoor-Baltork, Iraj; Sadeghi, Majid M.; Adibi, Abol-Hassan
Molecules, 2001 , vol. 6, # 11 p. 900 - 908
反应条件
oxygen; caesium carbonate; (-)-sparteine; PdCl2(nbd); 3 A molecular sieve in toluene; tert-butyl alcohol T=40°C; P=760 Torr; 18 h;
参考文献
Svenson, Doug; Kadla, John F.; Chang, Hou-Min; Jameel, Hasan
Canadian Journal of Chemistry, 2002 , vol. 80, # 7 p. 761 - 766
