(R)-(+)-3-苄氧基-1,2-丙二醇合成路线 (共 67 条)
反应条件
antimony trichloride in water; acetonitrile T=20°C; 0.166667 h;
参考文献
Wu, Qinpei; Wang, Yuan; Chen, Wei; Liu, Hua
Synthetic Communications, 2006 , vol. 36, # 10 p. 1361 - 1366
反应条件
1: With potassium hydroxide in benzene Etherification; 23 h; Heating; 2: With toluene-4-sulfonic acid in methanol; dichloromethane T=20°C; Ring cleavage; 5 h;
参考文献
Bhattacharya, Santanu; Dileep
Tetrahedron Letters, 1999 , vol. 40, # 46 p. 8167 - 8171
反应条件
hydrogenchloride in ethanol; chloroform; ethyl acetate; acetone
反应条件
sodium hydroxide; sulfuric acid in water
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=20°C; 2 h;
参考文献
Jana; Roy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 4 p. 707 - 709
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); potassium tert-butylate; hydrogen in tetrahydrofuran T=140°C; 4 h; Autoclave;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 52 p. 13041 - 13045
Angew. Chem., , vol. 124, # 52
反应条件
sodium phosphate buffer in di-isopropyl ether T=10°C; 24 h; Yields of byproduct given;
参考文献
Matsumoto, Kazutsugu; Fuwa, Seiji; Kitajima, Hidehiko
Tetrahedron Letters, 1995 , vol. 36, # 36 p. 6499 - 6502
反应条件
1: NaH 2: H2O / acetic acid View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 39 p. 7193 - 7196
反应条件
lithium amide; ammonia in tetrahydrofuran 0.166667 h;
参考文献
Chandrasekhar; Srinivas, Ch.; Srihari
Synthetic Communications, 2003 , vol. 33, # 6 p. 895 - 902
反应条件
sodium tetrahydroborate in ethanol; dichloromethane T=0°C; Reduction; 0.333333 h;
参考文献
European Journal of Organic Chemistry, , # 7 p. 1671 - 1678