(R)-(+)-3-苄氧基-1,2-丙二醇合成路线 (共 67 条)
反应条件
iodine; magnesium; ethylene dibromide 1.) 2-methyltetrahydrofuran, 45 min, 2.) - 15 deg C - room temperature, 120 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 25, # 24 p. 3993 - 4000
反应条件
in N,N-dimethyl-formamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, , vol. 47, # 6 p. 617 - 619
反应条件
in N,N-dimethyl-formamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, , vol. 47, # 6 p. 617 - 619
反应条件
Tetrabutyl-1,3-diisothiocyanato-distannoxane in methanol 1 h; Ambient temperature;
参考文献
Otera, Junzo; Nozaki, Hitosi
Tetrahedron Letters, 1986 , vol. 27, # 47 p. 5743 - 5746
参考文献
Tetrahedron Letters, , vol. 22, # 29 p. 2819 - 2822
反应条件
(i) NaOMe, MeOH, benzene, toluene, (ii) /BRN= 471308/; Multistep reaction;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 43, p. 2054 - 2061
反应条件
di(n-butyl)tin oxide; cesium fluoride multistep reaction; reaction with benzyl bromide; effect of differnt amounts of benzyl halides and CsF; effect of different reaction times and temperatures; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 8 p. 1972 - 1982
参考文献
DE403050 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1444
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C; 8 h; Yield given. Title compound not separated from byproducts;
参考文献
El'perina, E. A.; Struchkova, M. I.; Serkebaev, M. I.; Serebryakov, E. P.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 744 - 750
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 776 - 781
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C; 8 h; Yield given. Title compound not separated from byproducts;
参考文献
El'perina, E. A.; Struchkova, M. I.; Serkebaev, M. I.; Serebryakov, E. P.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 744 - 750
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 776 - 781