9-氯-9-氧代壬酸甲酯合成路线 （共 42 条）
反应条件
1: 70 percent / stannic chloride / benzene / 2 h / Ambient temperature 2: BF3(OC2H5)3 / CHCl3 / Ambient temperature 3: W6 Raney nickel / ethanol / Heating View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
反应条件
sodium tetrahydroborate
参考文献
Kallury, R. Krishnamohanrao; Krull, Ulrich J.; Thompson, Michael
Journal of Organic Chemistry, 1987 , vol. 52, # 24 p. 5478 - 5480
反应条件
sodium tetrahydroborate in 1,4-dioxane
参考文献
Beau, Jean-Marie; Aburaki, Shimpei; Pougny, Jean-Rene; Sinay, Pierre
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 621 - 622
反应条件
1: 15 g / aq. NH3 / 0 °C 2: Br2; CH3ONa / 0.25 h / Heating 3: 8.1 g / aq. HCl / 7 h / Heating View Scheme
参考文献
Petrenko; Petukhova; Shakirov; Shul'ts; Tolstikov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 7 p. 982 - 995
反应条件
1: sodium hydride / benzene / 2 h / Heating 2: 1.) hydrogen gas / 1.) 10percent palladium on charcoal / 1.) 95percent ethyl alcohol, 24 h; 2.) 95percent ethyl alcohol, reflux, 2 h 3: 94 percent / sodium methoxide / toluene / 0.5 h / Heating View Scheme
参考文献
Naora, Hirokazu; Ohnuki, Takashi; Nakamura, Asao
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 3 p. 993 - 994
反应条件
sodium tetrahydroborate
参考文献
Kallury, R. Krishnamohanrao; Krull, Ulrich J.; Thompson, Michael
Journal of Organic Chemistry, 1987 , vol. 52, # 24 p. 5478 - 5480
反应条件
1: triethylamine; diethyl ether / Erwaermen des Reaktionsprodukts mit wss.-aethanol. Kalilauge. 2: amalgamated zinc; aqueous hydrochloric acid View Scheme
参考文献
Canonica; Bacchetti
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1953 , vol. <8>15, p. 278,281
反应条件
1: 65 percent / stannic chloride / benzene / 2 h / Ambient temperature 2: BF3(OC2H5)3 / CHCl3 / Ambient temperature 3: W6 Raney nickel / ethanol / Heating 4: LAH / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
反应条件
1: 65 percent / stannic chloride / benzene / 2 h / Ambient temperature 2: BF3(OC2H5)3 / CHCl3 / Ambient temperature 3: W6 Raney nickel / ethanol / Heating View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
反应条件
1: 65 percent / stannic chloride / benzene / 2 h / Ambient temperature 2: BF3(OC2H5)3 / CHCl3 / Ambient temperature 3: W6 Raney nickel / ethanol / Heating View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
