9-氯-9-氧代壬酸甲酯合成路线 （共 42 条）
反应条件
polymer(resin Amberlyst A-26)-supported tetracarbonylhydridoferrate anion in tetrahydrofuran
1 h; Heating;
参考文献
Cainelli, Gianfranco; Manescalchi, Francesco; Umani-Ronchi, Achille
Journal of Organometallic Chemistry, 1984 , vol. 276, # 2 p. 205 - 208
反应条件
cadmium (II) chloride in diethyl ether
参考文献
Brandt,R.; Djerassi,C.
Helvetica Chimica Acta, 1968 , vol. 51, p. 1750 - 1762
反应条件
(i) CuI, Et2O, (ii) /BRN= 1775767/; Multistep reaction;
参考文献
Trost,B.M. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 4887 - 4902
反应条件
(i) 2-methoxybenzoic acid, Et3N, THF, (ii) /BRN= 3587200/; Multistep reaction;
参考文献
Terasawa,T.; Okada,T.
Tetrahedron, 1977 , vol. 33, p. 595 - 598
反应条件
diethyl ether; triethylamine
Erwaermen des Reaktionsprodukts mit wss.-aethanol. Kalilauge.;
参考文献
Blomquist et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4203
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Canonica; Bacchetti
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1953 , vol. <8>15, p. 278,281
反应条件
1: 47 percent / stannic chloride / various solvent(s) / 15 h / Ambient temperature
2: NaBH4 / methanol / 0.25 h
3: 82 percent / toluene-p-sulphonic acid / benzene / 2 h / Ambient temperature
View Scheme
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
反应条件
1: NaBH4 / dioxane
2: NIS, Ph3P / CH2Cl2
View Scheme
参考文献
Beau, Jean-Marie; Aburaki, Shimpei; Pougny, Jean-Rene; Sinay, Pierre
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 621 - 622
反应条件
1: 65 percent / stannic chloride / benzene / 2 h / Ambient temperature
2: BF3(OC2H5)3 / CHCl3 / Ambient temperature
3: W6 Raney nickel / ethanol / Heating
4: LAH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
反应条件
1: 60 percent / stannic chloride / benzene / 2 h / Ambient temperature
2: BF3(OC2H5)3 / CHCl3 / Ambient temperature
3: W6 Raney nickel / ethanol / Heating
4: LAH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 208 - 211
反应条件
1: 25.7 percent / SnCl4 / CHCl3 / 6 h / -50 °C
2: hydrazinhydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
3: diethyl ether
View Scheme
参考文献
Schoedel, Rolf; Spiteller, Gerhard
Helvetica Chimica Acta, 1985 , vol. 68, p. 1624 - 1634
