in various solvent(s) T=-78°C; 1 h;

lithium iodide in various solvent(s) -78 deg C, 1 h, -78-0 deg C, 1 h;

lithium bromide in tetrahydrofuran a soln. of dry LiBr in THF was added at 20°C under N2 to a stirred suspn. of CuBr in THF, soln. was cooled to -60°C and a soln. of t-BuMgCl in THF was added dropwise, mixt. was stirred for 15 min at -60°C; not isolated from the soln., used directly for further reactions;

暂无反应条件数据

N,N,N',N',N'',N''-hexamethylphosphoric triamide; chloro-trimethyl-silane; lithium iodide in various solvent(s) T=-78°C; 0.1 h;

in tetrahydrofuran 18 h; Ambient temperature;

lithium iodide in various solvent(s) T=-78°C; 1 h;