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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5659-33-6
合成路线
（共 24 条）
591-50-4
碘苯
+
3297-64-1
→
反应条件
5659-33-6
反应条件
Ag2CO3; caesium carbonate; PCy3∙HBF4; palladium (II) bromide in 1,4-dioxane T=150°C; 12 h; Inert atmosphereSealed tube;
参考文献
Rouchet, Jean-Baptiste; Schneider, Cedric; Spitz, Cedric; Lefevre, Johan; Dupas, George; Fruit, Corinne; Hoarau, Christophe
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3610 - 3615
108-86-1
溴代苯
+
3297-64-1
→
反应条件
5659-33-6
反应条件
copper(I) oxide; caesium carbonate; PCy3∙HBF4; palladium (II) bromide in 1,4-dioxane T=150°C; 12 h; Inert atmosphereSealed tube;
参考文献
Rouchet, Jean-Baptiste; Schneider, Cedric; Spitz, Cedric; Lefevre, Johan; Dupas, George; Fruit, Corinne; Hoarau, Christophe
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3610 - 3615
53744-31-3
→
反应条件
5659-33-6
反应条件
tin; ammonium chloride in ethanol; water 20 h; Reflux;
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
7473-93-0
2-硝基查耳酮
→
反应条件
5659-33-6
反应条件
sodium hydroxide; bakers' yeast in ethanol; water 1 h; Heating;
参考文献
Baik, Woonphil; Kim, Dong Ik; Lee, Hyun Joo; Chung, Wook-Jin; Kim, Byeong Hyo; Lee, Seok Woo
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4579 - 4580
53744-31-3
→
反应条件
612-96-4
2-苯基喹啉
+
5659-33-6
反应条件
tin; ammonium chloride in ethanol; water 26 h; Reflux;
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
93-10-7
喹哪啶酸
→
反应条件
5659-33-6
反应条件
1: trifluoroacetic anhydride; urea hydrogen peroxide addition compound / dichloromethane / 1.5 h / 0 - 20 °C 2: caesium carbonate; PCy3∙HBF4; palladium (II) bromide; copper(I) oxide / 1,4-dioxane / 12 h / 150 °C / |Inert atmosphere; |Sealed tube View Scheme
参考文献
Rouchet, Jean-Baptiste; Schneider, Cedric; Spitz, Cedric; Lefevre, Johan; Dupas, George; Fruit, Corinne; Hoarau, Christophe
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3610 - 3615
98-86-2
苯乙酮
→
反应条件
5659-33-6
反应条件
1: sodium carbonate / ethanol; water / 17 h / 20 °C 2: ammonium chloride; zinc / ethanol; water / 5 h / 60 °C View Scheme
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
552-89-6
邻硝基苯甲醛
→
反应条件
5659-33-6
反应条件
1: sodium carbonate / ethanol; water / 17 h / 20 °C 2: ammonium chloride; zinc / ethanol; water / 5 h / 60 °C View Scheme
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
98-86-2
苯乙酮
→
反应条件
612-96-4
2-苯基喹啉
+
5659-33-6
反应条件
1: sodium carbonate / ethanol; water / 17 h / 20 °C 2: hydrogenchloride; iron / ethanol; water / 12 h / 20 °C View Scheme
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
552-89-6
邻硝基苯甲醛
→
反应条件
612-96-4
2-苯基喹啉
+
5659-33-6
反应条件
1: sodium carbonate / ethanol; water / 17 h / 20 °C 2: hydrogenchloride; iron / ethanol; water / 12 h / 20 °C View Scheme
参考文献
Okuma, Kentaro; Seto, Jun-Ichi; Nagahora, Noriyoshi; Shioji, Kosei
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 6 p. 1372 - 1378
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