反应条件
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide
T=20°C; Heck reaction; 0.25 h;
2: 2-methoxy-6-bromo-naphthalene With Kaiser oxime-derived complex on resin base in N,N-dimethyl acetamide
T=120°C; Heck reaction; 14 h; Further stages. Title compound not separated from byproducts.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584