甲基 alpha-D-阿拉伯呋喃糖苷合成路线 （共 4 条）
参考文献
Sook, Jin Jun; Man, Sik Moon; So, Ha Lee; Chan, Seong Cheong; Kwan, Soo Kim
Tetrahedron Letters, 2005 , vol. 46, # 30 p. 5063 - 5065
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; Mitsunobu reaction; Inert atmosphere;
参考文献
Liu, Chunjuan; Richards, Michele R.; Lowary, Todd L.
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 4992 - 5007
反应条件
1: 51.1 percent / pyridine / 1.5 h / 0 - 55 °C
2: 27.4 percent / AcOH, HBr / 0.5 h / Ambient temperature
View Scheme
参考文献
Schneider; Engelhardt; Stobbe; Fenning; Chapman
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 7 p. 541 - 557
反应条件
1.1: Br2 / CCl4 / 4.5 h / 0 - 20 °C
1.2: 89 percent / pyridine / CCl4 / 1.5 h / 0 - 20 °C
2.1: pyridine / 0.08 h / 0 °C
3.1: n-Bu4NF*3H2O / tetrahydrofuran / 1 h
View Scheme
参考文献
Callam, Christopher S.; Gadikota, Rajendrakumar Reddy; Lowary, Todd L.
Carbohydrate Research, 2001 , vol. 330, # 2 p. 267 - 270
