2,3-二氢-1H-环戊并[b]喹啉合成路线 （共 24 条）
反应条件
T=750°C; P=0.01 Torr;
参考文献
Mao, Yuh-lin; Boekelheide, V.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1547 - 1548
反应条件
sulfuric acid in methanol
2.5 h; Irradiation;
参考文献
Olsen
Tetrahedron Letters, 1991 , vol. 32, # 39 p. 5235 - 5238
反应条件
zinc dibromide in chloroform
T=90 - 100°C; 2 h; Yield given;
参考文献
Koyama, Junko; Toyokuni, Izumi; Tagahara, Kiyoshi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 332 - 334
反应条件
1: 98 percent / p-Toluenesulfonic acid / benzene / Heating; Continuous removal of water
2: 36 percent / 750 °C / 0.01 Torr
View Scheme
参考文献
Mao, Yuh-lin; Boekelheide, V.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1547 - 1548
反应条件
1: 98 percent / p-Toluenesulfonic acid / benzene / Heating; Continuous removal of water
2: 36 percent / 750 °C / 0.01 Torr
View Scheme
参考文献
Mao, Yuh-lin; Boekelheide, V.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1547 - 1548
反应条件
in methanol
Irradiation;
参考文献
Austin, Mark; Egan, Oliver J.; Tully, Raymond; Pratt, Albert C.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 23 p. 3778 - 3786
反应条件
1: Pb(OCOCH3)4
2: ZnBr2 / CHCl3 / 2 h / 90 - 100 °C
View Scheme
参考文献
Koyama, Junko; Toyokuni, Izumi; Tagahara, Kiyoshi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 332 - 334
反应条件
in methanol
5 h; Irradiation;
参考文献
Austin, Mark; Egan, Oliver J.; Tully, Raymond; Pratt, Albert C.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 23 p. 3778 - 3786
反应条件
1.1: morpholine / toluene / Reflux
1.2: Reflux
2.1: palladium 10 on activated carbon; diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; acetic acid / 15 h / 120 °C / Inert atmosphere
View Scheme
参考文献
Xing, Rui-Guang; Li, Ya-Nan; Liu, Qiang; Han, Yi-Feng; Wei, Xia; Li, Jing; Zhou, Bo
Synthesis, 2011 , # 13 p. 2066 - 2072
反应条件
potassium hydroxide
Hydrogenation.an Palladium/Calciumcarbonat;
参考文献
Beer et al.
Journal of the Chemical Society, 1953 , p. 2440
