(S)-2-氨基-1-苯乙醇合成路线 （共 64 条）
反应条件
1: 77 percent / NH3 / ethanol / 18 h / 20 °C 2: 30 percent / LiAlH4 / tetrahydrofuran / 72 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 8 p. 1225 - 1233
反应条件
1.1: silver(l) oxide / dichloromethane / 0 - 20 °C 2.1: C10H18BNO; dimethylsulfide borane complex / tetrahydrofuran / 0 °C / Reflux 2.2: 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 2 art. no. P14610SS, p. 316 - 324
反应条件
1.1: sodium ethanolate / ethanol / 0.17 h / 20 °C 1.2: 1 h / 0 °C 2.1: silver(l) oxide / dichloromethane / 0 - 20 °C 3.1: C10H18BNO; dimethylsulfide borane complex / tetrahydrofuran / 0 °C / Reflux 3.2: 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 2 art. no. P14610SS, p. 316 - 324
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 46, # 5 p. 1653 - 1658
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
hydrogenchloride; sodium azide; water; hydrogen; palladium on activated charcoal 1.) DMF, 70 deg C, 48 h; 2.) ethanol, r.t.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3219 - 3222
反应条件
1: 93 percent / NaBH4 / ethanol / 6 h / 0 °C 2: 39 percent / 4 Angstroem sieves / hexane; tetrahydrofuran / 48 h / 25 °C / lipase from Pseudomonas cepacia 3: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
1: 84 percent / NaBH4 / ethanol / 6 h / 0 °C 2: 43 percent / 4 Angstroem sieves / diisopropyl ether / 36 h / 25 °C / lipase from Pseudomonas cepacia 3: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
