3,6-二碘-9-(4-甲基苯基)-9H-咔唑合成路线 （共 3 条）
反应条件
KIO3; acetic acid; potassium iodide
T=100°C; 1 h;
参考文献
Solvay SA
Patent: EP2433928 A1, 2012 ;
Location in patent: Page/Page column 10 ;
反应条件
1: potassium carbonate; copper / 18-crown-6 ether / 1,2-dichloro-benzene / 18 h / 178 °C / Inert atmosphere
2: potassium iodide; acetic acid; KIO3 / 1 h / 100 °C
View Scheme
参考文献
SOLVAY SA; MAUNOURY, Jonathan; ORSELLI, Enrico; FERRAND, Alexandre; BASCOUR, Dominique
Patent: WO2012/25510 A1, 2012 ;
反应条件
1: potassium carbonate; copper / 18-crown-6 ether / 1,2-dichloro-benzene / 18 h / 178 °C / Inert atmosphere
2: potassium iodide; acetic acid; KIO3 / 1 h / 100 °C
View Scheme
参考文献
SOLVAY SA; MAUNOURY, Jonathan; ORSELLI, Enrico; FERRAND, Alexandre; BASCOUR, Dominique
Patent: WO2012/25510 A1, 2012 ;
