N2,N2-二甲基-2,5-二氨基吡啶合成路线 (共 2 条)
反应条件
Pd/C; ammonium formate in methanol
0.5 h; Reflux;
参考文献
Nara, Susheel J.; Jha, Mukund; Brinkhorst, Johan; Zemanek, Tony J.; Pratt, Derek A.
Journal of Organic Chemistry, 2008 , vol. 73, # 23 p. 9326 - 9333
反应条件
1.1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / Inert atmosphere
1.2: 80 °C / Inert atmosphere
2.1: 10 palladium on activated charcoal; ammonium formate / methanol / Reflux
View Scheme
参考文献
Hanthorn, Jason J.; Valgimigli, Luca; Pratt, Derek A.
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 6908 - 6916