N-吡啶-2-甲基-甲酰胺合成路线 （共 10 条）
反应条件
trichlorophosphate; benzene
参考文献
Pfizer Inc.
Patent: US4097598 A1, 1978 ;
Title/Abstract Full Text Show Details
Pfizer Inc.
Patent: US4044015 A1, 1977 ;
反应条件
sodium hydroxide; formic acid in trichlorophosphate
参考文献
Pfizer Inc.
Patent: US4097598 A1, 1978 ;
反应条件
1: POCl3; benzene 2: CS2; AlCl3 View Scheme
参考文献
Bower; Ramage
Journal of the Chemical Society, 1955 , p. 2834,2836
反应条件
1: KH / tetrahydrofuran / 0 °C 2: KOH / methanol 3: Heating 4: 1.) n-BuLi / 1.) THF, -78 deg C, 1.5 h, 2.) -78 deg C-room temp. 5: hydrazine hydrate / ethanol; acetic acid / 25 °C View Scheme
参考文献
Meyers; Marra
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5863 - 5866
反应条件
1: N-(2-pyridylmethyl)formamide With sodium hydride in tetrahydrofuran 0.25 h; Inert atmosphere; 2: methyl iodide With sodium hydroxide in tetrahydrofuran Inert atmosphere;
参考文献
Hitomi, Yutaka; Hiramatsu, Kazuaki; Arakawa, Kengo; Takeyasu, Toshiyuki; Hata, Masashi; Kodera, Masahito
Dalton Transactions, 2013 , vol. 42, # 36 p. 12878 - 12882
反应条件
1: KH / tetrahydrofuran / 0 °C 2: KOH / methanol View Scheme
参考文献
Meyers; Marra
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5863 - 5866
反应条件
zinc oxide
T=70°C; 1 h;
参考文献
Hosseini-Sarvari, Mona; Sharghi, Hashem
Journal of Organic Chemistry, 2006 , vol. 71, # 17 p. 6652 - 6654
参考文献
Pfizer Inc.
Patent: US4282242 A1, 1981 ;
参考文献
Ko, Sangwon; Han, Hoon; Chang, Sukbok
Organic Letters, 2003 , vol. 5, # 15 p. 2687 - 2690
参考文献
Meyers; Marra
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5863 - 5866
