DL-2-氨基-1-环己醇合成路线 （共 10 条）
反应条件
ethanol; nickel T=50°C; P=110326 - 147102 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 3040
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Justus Liebigs Annalen der Chemie, , vol. 593, p. 81,87
Monatshefte fuer Chemie, , vol. 84, p. 1097
反应条件
ammonium hydroxide in o-xylene
参考文献
Journal of Organic Chemistry, , vol. 26, p. 3681 - 3685
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1230 - 1236
反应条件
2: lithium alanate; THF View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 593, p. 81,87
反应条件
(i) MeCN, Cl2, (ii) H2O; Multistep reaction;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 311, p. 15 - 35
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=20°C; Purification / work up;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 59 ;
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 24 h; CoolingInert atmosphere;
参考文献
Kang, Byungman; Miller, Aaron W.; Goyal, Sandra; Nguyen, Sonbinh T.
Chemical Communications, 2009 , # 26 p. 3928 - 3930
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile
T=20°C; Purification / work up;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 59 ;
反应条件
potassium hydroxide in ethanol
Heating;
参考文献
Shankaran; Donnelly, Karla L.; Shah, Shrenik K.; Guthikonda, Ravindra N.; MacCoss, Malcolm; Humes, John L.; Pacholok, Stephen G.; Grant, Stephan K.; Kelly; Wong
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 17 p. 4539 - 4544
