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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5665-83-8
合成路线
（共 21 条）
17049-49-9
正辛基镁溴盐
+
18431-79-3
→
反应条件
6836-42-6
6-十四烷酮
+
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF - diethyl ether, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
920-39-8
异丙基溴化镁
+
67532-01-8
→
反应条件
923-28-4
正戊基异丙基甲酮
+
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
1589-82-8
苄基溴化镁
+
67532-01-8
→
反应条件
6683-94-9
1-苯基-2-庚酮
+
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
693-25-4
正戊基溴化镁
+
67532-01-8
→
反应条件
927-49-1
二正戊基酮
+
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
693-25-4
正戊基溴化镁
+
18431-79-3
→
反应条件
927-49-1
二正戊基酮
+
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF - diethyl ether, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
14572-78-2
→
反应条件
5665-83-8
反应条件
sodium hydroxide; dihydrogen peroxide Ambient temperature; Yield given;
参考文献
Pelter, Andrew; Rao, J. Madhusudhana
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1149 - 1150
67532-02-9
+
931-50-0
环己基溴化镁
→
反应条件
5665-83-8
+
90542-50-0
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
67532-01-8
+
1730-25-2
烯丙基溴化镁
→
反应条件
5665-83-8
+
61168-10-3
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
18431-79-3
+
1730-25-2
烯丙基溴化镁
→
反应条件
5665-83-8
+
61168-10-3
反应条件
sodium hydroxide; dihydrogen peroxide 1) THF - diethyl ether, -50 deg C, 1 h, 2) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
42126-51-2
→
反应条件
5665-83-8
反应条件
(i) MeSO3H, (MeOCH2CH2)2O, (ii) aq. H2O2; Multistep reaction;
参考文献
Pelter,A. et al.
Journal of the Chemical Society, Chemical Communications, 1973 , p. 544 - 545
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