2-溴-5-甲氧基苯甲酰氯合成路线 （共 16 条）
反应条件
thionyl chloride 18 h; Heating;
参考文献
Hellwinkel, Dieter; Bohnet, Siegbert
Chemische Berichte, 1987 , vol. 120, p. 1151 - 1174
反应条件
N,N-dimethyl-formamide in dichloromethane
参考文献
US2003/55085 A1, ;
US 20030055085 A1
反应条件
1: 95 percent / Br2 / acetic acid 2: 98 percent / SOCl2 / 18 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 120, p. 1151 - 1174
反应条件
1: 31 percent / KMnO4 2: 95 percent / Br2 / acetic acid 3: 98 percent / SOCl2 / 18 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 120, p. 1151 - 1174
参考文献
Nielsen, Simon F.; Larsen, Mogens; Boesen, Thomas; Schonning, Kristian; Kromann, Hasse
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2667 - 2677
反应条件
in tetrahydrofuran T=20°C; 16 h;
参考文献
Woodward, David F.; Martos, Jose L.; Carling, William R.; Poloso, Neil J.; Wang, Jenny W.
Patent: US2012/270915 A1, 2012 ;
Location in patent: Page/Page column 20 ;
US 20120270915 A1
反应条件
in toluene T=0 - 20°C; 0.5 h;
参考文献
Genelabs Technologies, Inc.
Patent: US2007/32488 A1, 2007 ;
Location in patent: Page/Page column 28-29 ;
反应条件
n-butyllithium; sulfuric acid Yield given. Multistep reaction;
参考文献
Barraclough, Paul; Smith, Steven
Journal of Chemical Research, Miniprint, 1995 , # 2 p. 526 - 541
反应条件
Yield given. Multistep reaction;
参考文献
Hellwinkel, Dieter; Bohnet, Siegbert
Chemische Berichte, 1987 , vol. 120, p. 1151 - 1174
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Furuta, Takumi; Kitamura, Yuki; Hashimoto, Ayano; Fujii, Satoshi; Tanaka, Kiyoshi; Kan, Toshiyuki
Organic Letters, 2007 , vol. 9, # 2 p. 183 - 186
