苯甲酰甲基-二甲基-溴化硫合成路线 (共 18 条)
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 6 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 708 - 712
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 828 - 833
反应条件
1: 90 percent / aq. NaOH / 0.83 h 2: 70 percent / NH4OAc / acetic acid / 6 h / Heating View Scheme
参考文献
Tewari, Ram S.; Awasthi, Alok K.
Synthesis, 1981 , # 4 p. 314 - 315
反应条件
in various solvent(s) 4 h; Heating;
参考文献
Gupta, K. C.; Manglum, P.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 223 - 225
反应条件
in various solvent(s) 4 h; Heating;
参考文献
Gupta, K. C.; Manglum, P.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 223 - 225
反应条件
beim Versetzen der Reaktionsloesung mit wss. H2SO4;
参考文献
Boehme; Krause
Chemische Berichte, 1949 , vol. 82, p. 426,431,432
反应条件
in various solvent(s) 4 h; Heating;
参考文献
Gupta, K. C.; Manglum, P.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 223 - 225
反应条件
1: 90 percent / aq. NaOH / 0.83 h 2: 62 percent / NH4OAc / acetic acid / 6 h / Heating View Scheme
参考文献
Tewari, Ram S.; Awasthi, Alok K.
Synthesis, 1981 , # 4 p. 314 - 315
反应条件
1: 2-phenyl-2-oxoethyldimethylsulfonium bromide With caesium carbonate in anhydrous xylene
T=20°C;
2: N-(2-(chloromethyl)phenyl)-4-methylbenzenesulfonamide in anhydrous xylene
T=20°C;
参考文献
Yang, Qing-Qing; Xiao, Cong; Lu, Liang-Qiu; An, Jing; Tan, Fen; Li, Bin-Jie; Xiao, Wen-Jing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 36 p. 9137 - 9140
反应条件
sodium hydride
1.) DMSO, rt., both educts were treated separately with reagent; 2.) DMSO, 80 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; La Rosa, Concetta
Heterocycles, 1996 , vol. 43, # 11 p. 2397 - 2407
反应条件
in various solvent(s)
4 h; Heating;
参考文献
Gupta, K. C.; Manglum, P.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 223 - 225