1,1'-[氧基二(亚甲基)]二(4-硝基苯)合成路线 (共 17 条)
反应条件
sulfuric acid; PFC in water; acetic acid T=39.9°C; MechanismRate constant;
参考文献
Jagathesan, A.; Nambi, K.; Arulraj, S. J.; Ahamed, K. A. Basheer
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1989 , vol. 28, # 10 p. 904 - 905
反应条件
sulfuric acid; PFC in water; acetic acid T=39.9°C; MechanismRate constant;
参考文献
Jagathesan, A.; Nambi, K.; Arulraj, S. J.; Ahamed, K. A. Basheer
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1989 , vol. 28, # 10 p. 904 - 905
反应条件
calcium persulfate; silica gel
0.166667 h; microwave irradiation;
参考文献
Badri, Rashid; Kiasat, Ali Reza; Nazari, Simin
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 3 p. 589 - 593
反应条件
sulfuric acid; silica gel in hexane
T=20°C; 0.5 h;
参考文献
Shokrollahi, Arash; Zali, Abbas; Pouretedal, Hamid Reza
Synthetic Communications, 2008 , vol. 38, # 3 p. 371 - 375
反应条件
1: (4-nitro-phenyl)-methanol With sodium hydride in N,N-dimethyl-formamide; mineral oil
Cooling with ice;
2: 1-bromomethyl-4-nitro-benzene With sodium iodide in N,N-dimethyl-formamide; mineral oil
参考文献
Banerjee, Moloy; Farahat, Abdelbasset A.; Kumar, Arvind; Wenzler, Tanja; Brun, Reto; Munde, Manoj M.; Wilson, W. David; Zhu, Xiaohua; Werbovetz, Karl A.; Boykin, David W.
European Journal of Medicinal Chemistry, 2012 , vol. 55, p. 449 - 454
反应条件
1,1,3,3-tetramethyldisiloxane; trimethylsilyl trifluoromethanesulfonate
T=-78°C; 1.16667 h;
参考文献
Aizpurua, Jesus M.; Lecea, Begona; Palomo, Claudio
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2342 - 2347
反应条件
Nafion-H
T=90 - 95°C; 24 h;
参考文献
Yamato, Takehiko; Hideshima, Chieko; Prakash, G. K. Surya; Olah, George A.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2089 - 2091
反应条件
tetrafluoroboric acid in dichloromethane
0.166667 h;
参考文献
Takadate, Akira; Tahara, Tsutom; Goya, Shujiro
Synthesis, 1983 , # 10 p. 806 - 807
反应条件
N,N-dimethylbenzylamine oxide-SbCl5 in nitromethane
2 h; Heating;
参考文献
Yamamoto, Jiro; Tanioka, Yukio; Umezu, Masahiro
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 9 p. 3035 - 3036
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
1 h; Further byproducts given;
参考文献
Kam, Toh-Seok; Lim, Tuck-Meng
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 2 p. 147 - 150