顺式-11-十六烯-1-醇合成路线 （共 65 条）
反应条件
1: 97 percent / H2 / Lindlar Catalyst / quinoline; heptane / 0 °C 2: 96 percent / LiAlH4 / diethyl ether / 5 h View Scheme
参考文献
Chemische Berichte, , vol. 113, # 12 p. 3898 - 3903
反应条件
1: KOH / methanol / 24 h / Heating 2: 97 percent / H2 / Lindlar Catalyst / quinoline; heptane / 0 °C 3: 96 percent / LiAlH4 / diethyl ether / 5 h View Scheme
参考文献
Chemische Berichte, , vol. 113, # 12 p. 3898 - 3903
反应条件
1: 1) NaH, ethylenediamine / 1) benzene, 60 deg C, 2) 60 deg C, 2h 2: 90 percent / p-TsOH / CH2Cl2 / Ambient temperature 3: LiNH2 / liquid ammonia 4: p-TsOH / methanol 5: 87 percent / H2 / P2Ni View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 755 - 756
反应条件
1: 1) LiNH2 / 1) NH3, 2) THF 2: 1) NaH, ethylenediamine / 1) benzene, 60 deg C, 2) 60 deg C, 2h 3: 90 percent / p-TsOH / CH2Cl2 / Ambient temperature 4: LiNH2 / liquid ammonia 5: p-TsOH / methanol 6: 87 percent / H2 / P2Ni View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 755 - 756
反应条件
1: 86 percent / p-toluenesulphonic acid / benzene / 8 h / 120 °C 3: 86 percent / dil. HCl / diethyl ether / 2.5 h / Ambient temperature 4: 0.91 g / NaBH4 / methanol / 2 h / 0 °C View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 757 - 759
反应条件
1: LiNH2 / liquid ammonia 2: p-TsOH / methanol 3: 87 percent / H2 / P2Ni View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 755 - 756
反应条件
1: pyridine / Ambient temperature 3: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h 4: 97 percent / 10percent aq. sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4514 - 4517
反应条件
2: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h 3: 97 percent / 10percent aq. sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4514 - 4517
反应条件
1: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h 2: 97 percent / 10percent aq. sodium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4514 - 4517
反应条件
9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran
参考文献
Chemische Berichte, , vol. 111, # 1 p. 248 - 253
