顺式-11-十六烯-1-醇合成路线 (共 65 条)
反应条件
1: 55 percent / Li2CuCl4 / tetrahydrofuran / 3 h / -10 °C 2: 52 percent / pyridinium p-toluenesulfonate / methanol / 6 h / 55 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 29, # 6 p. 518 - 520
反应条件
1: (i) Na<N(SiMe3)2>, THF, (ii) /BRN= 1746480/ 2: 9-BBN / tetrahydrofuran View Scheme
参考文献
Chemische Berichte, , vol. 111, # 1 p. 248 - 253
反应条件
sodium hydride; dimethyl sulfoxide in tetrahydrofuran 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Agricultural and Biological Chemistry, , vol. 44, # 2 p. 257 - 261
反应条件
1: 1) O3, 2) NaBH4 / 1) cyclohexane, MeOH 2: 92 percent / i-BuMgBr, Cp2TiCl2 View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 33, # 1 p. 25 - 30
反应条件
sodium amide 1.) THF, 25 deg C, 30 min, 2.) -80 deg C to 25 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 26, # 3 p. 307 - 310
反应条件
9-borabicyclo[3.3.1]nonane dimer; acetic acid 1.) THF, 0-5 deg C, 24 h, 2.) reflux, 9 h; Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 609 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 671 - 672
反应条件
1: 85 percent 2: 1) O3, 2) NaBH4 / 1) cyclohexane, MeOH 3: 92 percent / i-BuMgBr, Cp2TiCl2 View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 33, # 1 p. 25 - 30
反应条件
1: 95 percent / 6.5 h / -5 - 0 °C View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 18, # 2 p. 219 - 224
Khimiya Prirodnykh Soedinenii, , vol. 18, # 2 p. 239 - 245
参考文献
Chemistry of Natural Compounds, , vol. 18, # 2 p. 219 - 224
Khimiya Prirodnykh Soedinenii, , vol. 18, # 2 p. 239 - 245
反应条件
pyridine 12 h; Ambient temperature;
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 116 - 118
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 132 - 135