4'-羧基苯并-15-冠5-醚合成路线 (共 11 条)
反应条件
chromium(VI) oxide; sulfuric acid 0.416667 h;
参考文献
Gunter, Maxwell J.; Johnston, Martin R.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 8 p. 1009 - 1018
反应条件
sodium hydroxide; bromine in water T=0 - 10°C;
参考文献
Haines, Alan H.; Hodgkisson, Ian; Smith, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 311 - 318
反应条件
sodium acetate; palladium diacetate in acetonitrile P=6619.6 Torr; 1 h; Ambient temperature;
参考文献
Nagira, Kazuhiko; Kikukawa, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2365 - 2368
反应条件
1: NaOH / ethanol / 48 h / Heating 2: KMnO4 / H2O View Scheme
参考文献
Chemical Communications, , # 14 p. 1291 - 1292
反应条件
1: thionyl chloride / dimethylformamide / 6 h / Heating 2: NaOH / ethanol / 48 h / Heating 3: KMnO4 / H2O View Scheme
参考文献
Chemical Communications, , # 14 p. 1291 - 1292
反应条件
in potassium hydroxide; ethanol 24 h; Heating;
参考文献
Fu, Enqin; Granell, Jaume; Green, Malcolm L.H.; Lowe, Valerie J.; Marder, Seth R.; et al.
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 205 - 218
反应条件
1: 46 percent / aq. NaOH / butan-1-ol 2: 75 percent / Br2, aq. NaOH View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 6 p. 1593 - 1598
反应条件
lithium hydroxide; lithium chloride in ethanol; water T=25°C; other substrates; Rate constantMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 5 p. 579 - 582
反应条件
1: 54 percent / dimethylsulfoxide / 8 h / Heating 2: 66 percent / ethanol; aq. KOH / 24 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 355, p. 205 - 218
反应条件
1: 65 percent / P2O5, CH3SO3H / 6 h 2: 83 percent / aq. NaOH, Br2 / 5 h / 20 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 72, # 7 p. 1614 - 1620