4'-甲氧基羰基苯并-15-冠5-醚合成路线 （共 5 条）
反应条件
potassium carbonate in acetonitrile 24 h; Heating;
参考文献
He, Chunlin; Shi, Zuming; Zhou, Qizhong; Li, Shijun; Li, Ning; Huang, Feihe
Journal of Organic Chemistry, 2008 , vol. 73, # 15 p. 5872 - 5880
反应条件
pyridine 18 h; Ambient temperature;
参考文献
Haines, Alan H.; Hodgkisson, Ian; Smith, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 311 - 318
反应条件
1: 89 percent / bromine, sodium hydroxide / H2O / 0 - 10 °C 2: 99 percent / oxalyl chloride, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: 80 percent / pyridine / 18 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 311 - 318
反应条件
1: 99 percent / oxalyl chloride, pyridine / CH2Cl2 / 4 h / Ambient temperature 2: 80 percent / pyridine / 18 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 311 - 318
反应条件
1: 75 percent / sodium carbonate, potassium permanganate / H2O / 1.) 0 deg C, 2 h, 2.) room temperature, 12 h 2: 99 percent / oxalyl chloride, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: 80 percent / pyridine / 18 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 311 - 318
