1,1,1,3-四氯十一烷合成路线 (共 6 条)
反应条件
potassium carbonate; palladium diacetate; triphenylphosphine
120 h; Ambient temperatureinvestigation of catalyzed addition reaction of polyhaloalkanes to olefins; variation of reagent, catalyst, temperature and atmosphere; Product distribution;
参考文献
Tsuji, Jiro; Sato, Koji; Nagashima, Hideo
Chemistry Letters, 1981 , p. 1169 - 1170
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in benzene
T=140°C; 36 h;
参考文献
Kamigata, Nobumasa; Sawada, Hideo; Suzuki, Norihiro; Kobayashi, Michio
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 199 - 204
反应条件
Cr(acetylacetone)3; water
T=170°C; 6 h; Autoclave;
参考文献
Khusnutdinov; Schadneva; Oshnyakova; Dzhemilev
Petroleum Chemistry, 2009 , vol. 49, # 4 p. 331 - 338
反应条件
CuCl2·2H2O; Cr(acetylacetone)3; water
T=150 - 160°C; Sealed tube;
参考文献
Khusnutdinov; Oshnyakova; Shchadneva
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1428 - 1432
Zhurnal Organicheskoi Khimii, 2013 , vol. 49, # 10 p. 1451 - 1455,5
反应条件
tetrachloromethane; Cr(acetylacetone)3
T=170°C; 6 h; Autoclave;
参考文献
Khusnutdinov; Schadneva; Oshnyakova; Dzhemilev
Petroleum Chemistry, 2009 , vol. 49, # 4 p. 331 - 338
反应条件
RuCl2(p-cymene)(N,N-dimesyl-4,5-dichloroimidazole) in N-dodecane; toluene
T=90°C; 60 h; Product distribution; Further Variations:reaction times;
参考文献
Richel, Aurore; Delfosse, Sebastien; Cremasco, Cedric; Delaude, Lionel; Demonceau, Albert; Noels, Alfred F.
Tetrahedron Letters, 2003 , vol. 44, # 32 p. 6011 - 6015