2,5-二溴-N-正辛基-3,4-噻吩二甲酰亚胺合成路线 （共 11 条）
反应条件
N-bromosuccinmide in sulfuric acid; trifluoroacetic acid T=20°C;
参考文献
Zou, Yingping; Najari, Ahmed; Berrouard, Philippe; Beaupre, Serge; Reda Aich, Badrou; Tao, Ye; Leclerc, Mario
Journal of the American Chemical Society, 2010 , vol. 132, # 15 p. 5330 - 5331
反应条件
1: 86 percent / Ac2O / 140 °C 2: 85 percent / toluene / 24 h / Heating 3: 79 percent / SOCl2 / 3 h / Heating 4: 81 percent / NBS / aq. H2SO4; trifluoroacetic acid / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 19 p. 3381 - 3384
反应条件
1: in tetrahydrofuran T=50°C; 3 h; Inert atmosphere; 2: With thionyl chloride in tetrahydrofuran T=55°C; 4 h; Inert atmosphere;
参考文献
Cabanetos, Clement; El Labban, Abdulrahman; Bartelt, Jonathan A.; Douglas, Jessica D.; Mateker, William R.; Frechet, Jean M. J.; McGehee, Michael D.; Beaujuge, Pierre M.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4656 - 4659
反应条件
1: 79 percent / SOCl2 / 3 h / Heating 2: 81 percent / NBS / aq. H2SO4; trifluoroacetic acid / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 19 p. 3381 - 3384
反应条件
1: 85 percent / toluene / 24 h / Heating 2: 79 percent / SOCl2 / 3 h / Heating 3: 81 percent / NBS / aq. H2SO4; trifluoroacetic acid / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 19 p. 3381 - 3384
反应条件
1: 74 percent / KOH / ethane-1,2-diol / Heating 2: 86 percent / Ac2O / 140 °C 3: 85 percent / toluene / 24 h / Heating 4: 79 percent / SOCl2 / 3 h / Heating 5: 81 percent / NBS / aq. H2SO4; trifluoroacetic acid / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 19 p. 3381 - 3384
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide
参考文献
Organic Letters, , vol. 13, # 1 p. 38 - 41
反应条件
T=20 - 130°C; 0.5 h; Inert atmosphere;
参考文献
Braunecker, Wade A.; Owczarczyk, Zbyslaw R.; Garcia, Andres; Kopidakis, Nikos; Larsen, Ross E.; Hammond, Scott R.; Ginley, David S.; Olson, Dana C.
Chemistry of Materials, 2012 , vol. 24, # 7 p. 1346 - 1356
反应条件
1.1: acetic anhydride / |Inert atmosphere 2.1: tetrahydrofuran / 3 h / 50 °C / |Inert atmosphere 2.2: 4 h / 55 °C / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 12 p. 4656 - 4659
反应条件
1.1: acetic anhydride / 140 °C 1.2: 24 h / |Reflux 1.3: 12 h / |Reflux 2.1: N-bromosuccinmide; sulfuric acid; trifluoroacetic acid / 20 °C View Scheme
参考文献
Macromolecules, , vol. 45, # 17 p. 6906 - 6914,9
