1: [2-(4-Bromophenoxy)ethoxy](1,1-dimethylethyl)dimethylsilane With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
2: N,N-dimethyl-formamide in tetrahydrofuran; hexane
T=-78 - 20°C; 3 h;
3: With water in tetrahydrofuran; hexane
参考文献
MERCK FROSST CANADA LTD.
Patent: WO2007/9250 A1, 2007 ;
Location in patent: Page/Page column 59 ;
WO 2007/009250 A1