1: acetylacetone With sodium hydride in tetrahydrofuran
T=0°C; 5.5 h; Inert atmosphereSchlenk technique;
2: 1-bromomethyl-4-nitro-benzene in tetrahydrofuran
RefluxInert atmosphereSchlenk technique;
参考文献
Tregubov, Andrey A.; Vuong, Khuong Q.; Luais, Erwann; Gooding, J. Justin; Messerle, Barbara A.
Journal of the American Chemical Society, 2013 , vol. 135, # 44 p. 16429 - 16437