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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5670-65-5
合成路线
（共 6 条）
5670-65-5
+
75-86-5
丙酮氰醇
→
反应条件
反应条件
N,O-di[3,5-bis(trifluoromethyl)benzyl]cinchoninium bromide; potassium carbonate in toluene T=-30°C; 72 h; optical yield given as percent eeenantioselective reaction;
参考文献
Bernardi, Luca; Fini, Francesco; Fochi, Mariafrancesca; Ricci, Alfredo
Synlett, 2008 , # 12 p. 1857 - 1861
5670-65-5
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
zinc(II) tetrahydroborate in ethylene glycol dimethyl ether T=25°C; 9 h;
参考文献
Ranu; Chakraborty
Tetrahedron, 1992 , vol. 48, # 25 p. 5317 - 5322
5670-65-5
→
反应条件
59647-78-8
2-苯基丙醛肟
+
7796-75-0
+
746647-15-4
反应条件
glucose dehydrogenase; D-glucose; β-NADP+ T=30°C; pH=7.5; 24 h; aq. buffer; optical yield given as percent ee;
参考文献
Durchschein, Katharina; Ferreira-Da Silva, Bianca; Wallner, Silvia; MacHeroux, Peter; Kroutil, Wolfgang; Glueck, Silvia Maria; Faber, Kurt
Green Chemistry, 2010 , vol. 12, # 4 p. 616 - 619
5670-65-5
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
glucose dehydrogenase; D-glucose; pentaerythritol tetranitrate reductase from Enterobacter cloacae PB2; nicotinamide adenine dinucleotide T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
5670-65-5
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
glucose dehydrogenase; D-glucose; OPR3 isoenzyme of 12-oxophytodienoate reductase from Lycopersicon esculentum; NADP T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
5670-65-5
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
glucose dehydrogenase; xenobiotic reductase A from Pseudomonas putida; D-glucose; NADP T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
